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MECH 2300 MATERIALS I

 

 

 

 


1.   Lectures

The textbook by WD Callister, Jr: Materials Science and Engineering, 5th Edition will be used.

Dr A. Ruys will give lectures 1 to 16 and an end-of-term examination will be based on these lectures which counts for 50% of the written examination.

Professor MV Swain will present lectures 17 to 24 and an end-of-term examination will be based on these lectures which counts for 50% of the written examination.

Marking schemes:

Written examination

60%

Laboratory reports

20%

Tutorials and assignments

20%

Lecturers

Dr A. Ruys (ME Bldg Rm 521)                           a.ruys@aeromech.usyd.edu.au

Professor MV Swain (ME Bldg Rm 332)            mswain@aeromech.usyd.edu.au

Tutors / Demonstrators

Ms E. Kolos  (ME Bldg Rm 342)                       elizabeth.kolos@aeromech.usyd.edu.au

Mr P. Boughton (ME Bldg Rm 342)                   boughton@aeromech.usyd.edu.au

2.    Contents of Lectures:

Lecture

Description

1

Objectives, structure and assessment of the course.

2

General introduction to materials (Chapter 1)

3

Structure of crystalline solids (Chapter 3)

4

Imperfections in solids (Chapter 4)

5

Imperfections in solids (Cont'd Chapter 4)

6

Diffusion in solids and engineering applications (Chapter 5)

 

Assignment #1 due

7

Mechanical properties of metals (Chapter 6)

8

Dislocation and strengthening mechanisms (Chapter 7)

9

Dislocation and strengthening mechanisms (Cont'd Chapter 7)

10

Failure of solids (Chapter 8)

11

Failure of solids (Cont'd Chapter 8)

12

Failure of solids (Cont'd Chapter 8)

 

Assignment #2 due

13

Phase diagrams (Chapter 9)

14

Phase diagrams (Cont'd Chapter 9)

15

Annealing and heat treatment (Chapter 11)

16

Precipitation hardening (Cont'd Chapter 11)

17

TBA

18

 

Assignment #3 due

(Mid Semester Break)

19

(Prof Swain to provide contents of Lectures 17 - 24 based on Callister's book: Chapters 18, 19, 20, 21 and 22)

20

21

22

23

24

 

Assignment #4 due

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3.    Tutorial and Assignment

Attendance in tutorial classes is compulsory and will be recorded by the tutors. Marks (up to a maximum of 5) will be deducted from the final marks for tutorials/assignments. Tutorials have been timetabled for Tuesday and Thursdays as per listed below. These will commence in week 2.

Tuesdays 11:00 to 12:00               

MT3 (Tutor: P. Boughton)

                                                        

EE614 (Tutor: E. Kolos)

Wednesdays 11:00 to 12:00               

MT3 (Tutor: P. Boughton)

 

MT2 (Tutor: E. Kolos)

Thursdays 9:00 -10:00

MT3 (Tutor: P. Boughton)

 

MT4 (Tutor: E. Kolos)

Thursdays 10:00 -11:00

MT3 (Tutor: P. Boughton)

 

MT4 (Tutor: E. Kolos)

MT3 - Mechanical Engineering Tutorial Rm 3; EE614 - Electrical Engineering Tutorial Rm 614 etc

You should have the schedule for the tutorial classes and the deadline for the submission of assignments from the department already. Submit your assignment to your tutor who will mark them and return to you in two weeks.

The four tutorials 1, 2, 3, and 4 are all taken from the Callister Jr book: Materials Science and Engineering. Generally, you are given about three weeks to solve all the questions in each tutorial and you should attempt to finish them in class. Tutorial questions will not be marked but attendance is compulsory. Marks will be deducted for non-attendance. You will be given separate assignments A1, A2, A3 and A4 and you should hand them in to the respective tutors according to the assignment schedule. It is not always possible to arrange tutorials in phase with lectures and students will be told about reading materials before they come to the tutorial classes.


 

 

 

Start: 10 July

 

 

Finish: 28 July

 

      

Calister:

Chapter 3

Q3.4, Q3.6

 

 

Chapter 4

Q4.5, Q4.30

 


Read Chapters 3 and 4.

 

 

 

Dut date:  Friday 10 July

 

Calister:        

Chapter 3

Q3.8, Q3.18

                       

 

Chapter 4

Q4.21, Q4.31


 

 

Start: 31 July

 

Finish: 18 August

 

Calister:     

Chapter 5

Q5.7

 

                    

Chapter 6 

Q6.27

 

                    

Chapter 7

Q7.20, 7.25

 


Read Chapters 5, 6 and 7.

 

 

 

 

 

 

 

 

Dut date:  TBA

 

Calister:

Chapter 6

Q6.22, Q6.43

 

 

Chapter 7

Q7.18, Q7.32

 

                          

 

 

 


 

Start: 21 August

 

Finish: 1 September

 

Calister:      

Chapter 8

Q 8.5, Q8.32  

                    

 

Chapter 9

Q9.5, Q9.7

 


Read Chapters 8, 9 and 11.

 

Dut date:  TBA

 

Calister:

Chapter 8

Q 8.4, Q8.14

                       

 

Chapter 9

Q9.21, Q9.22

 


(Professor Swain will set Tutorial #4 and Assignment A4)

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4.     Experiments:

There are two laboratory experiments for each student, M1 and M2. You will be given a schedule of all these experiments when they are finalised. Each experiment will normally take one 3-hour afternoon. If additional time is required, arrangements can be made with the demonstrators. P. Boughton (M1) and E. Kolos  (M2) will be your demonstrators. They will be responsible to show you how to conduct the experiments and mark your laboratory reports which you have to hand in within 2 weeks after the experiments have been completed. Always observe safety rules in the laboratory as the testing machines and other facilities may cause bodily harm to you if not careful. Laboratory attendance is compulsory. Non-attendance will result in marks being deducted from the final score.


 

Materials Laboratory M1: Mechanical Properties of Engineering Materials
Venue: Materials Laboratory, Mechanical Engineering Building Room 163

Purposes of Experiment:

The main aims are:

(a) to help the students to have hands-on experience of standard mechanical testing machines to measure typical mechanical properties of materials;
(b) to understand why metals behave differently to polymers; and
(c) to determine and appreciate the significance of the ductile-brittle transition phenomenon in metals and polymers.

Materials for the Experiment:

Each group will choose one metal and one polymer for the experiment. The metals can be either a low carbon steel or an aluminium alloy. The polymers may be chosen from PVC, PMMA and Nylon etc depending on what is available in the Mechanical Engineering Workshop. Standard tensile and Charpy specimens will be manufactured by the ME Workshop and provided to students for testing. No need to manufacture hardness specimens as any of these two specimens is suitable for the hardness tests.

The Experiment:

The following tests should be performed:-
(a) Standard tensile tests to evaluate tensile modulus, yield strength, ultimate tensile strength, and elongation-to-break using the Insron 1195 universal testing machine. (45 minutes)
(b) Measure the Brinell (for metals) and Vicker (polymers) hardness numbers with the universal hardness tester. (30 minutes)
(c) Study the ductile-brittle transition behaviour (if any) using the Charpy impact testing machines for metals and polymers, respectively, in the laboratory. (45 minutes)

Laboratory Report:

Each student has to submit his/her own report and no group report will be accepted.

The report should contain the mechanical properties of the chosen materials and comparisons should be made. Comment on the relationships between hardness and tensile yield or ultimate strength for metals; as well as hardness and elastic modulus for polymers from these experimental results. Also the ductile-brittle transition phenomenon should be explained in relation to the microstructures. (eg hcp aluminium will not show this ductile-brittle transition). Discuss the fracture surfaces in relation to brittle cleavage and fibrous shear failures if possible. (In this case, you will need to examine the failure surfaces with an optical microscope in our laboratory or you may wish to go the EMU to use the SEM. In the latter case you will need the assistance of your demonstrator. This additional work will depend on your own initiative.)


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Materials Laboratory M2:- Weibull Strength of Brittle Materials
Venue: Materials Laboratory, Mechanical Engineering Building, Room 163

Purposes of Experiment:

The main aims are:

(a) to familiarise the students about the non-uniqueness of strength properties of brittle materials; and
(b) to bring to their attention the importance of Weibull strength theory and probability of failure.

Materials and Testing:

Microscopic glass slides about 1 mm thick will be used for three point-bending tests. From the load-deflection record calculate the Young's modulus and the bending strength. You need to test about 20 glass slides to get a reasonable sample size for Weibull analysis. Use the Instron 1195 testing machine with a displacement rate of about 10 mm/min. Make sure that no splints and broken pieces are left in the machine or fly apart everywhere. (60 minutes)

Take another 20 glass slides and treat them with hydrofluric acid (HF). Then repeat the bending tests. Calculate the Young's modulus and bending strength again. (60 minutes)

Laboratory Report:

Each student has to submit his/her laboratory report and there will be no group report.

In your laboratory report you should plot the bending strength versus frequency and Young's modulus versus frequency distribution curves. Use these results to determine the Weibull moduli for as-received glasses. Comment on the values of the Weibull moduli obtained from the Young's modulus and the bending strength results. Do you expect the Weibull moduli to be very different and why? Give the Weibull strength equation for the as-received glass slides tested.

Report the same as above for the glass slides that were treated with HF. Comment on the Young's modulus and bending strength distribution curves and their Weibull moduli. What do you think are the effects of the HF treatment? How does the bending strength distribution curve change?

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5. Unit of Study Description

 

MECH2300: Materials 1

 

Unit of Study Description (from the Engineering Handbook)

4 credit points.

Semester: 2.

Classes: 2 lec and 1 tut/week plus 2 laboratory sessions per student.

Prerequisite: None

Prohibition: CIVL2101 (students can enrol in either MECH2300 or CIVL2101, but not both)

Assessment: One 2 hr exam, assignments and laboratory work.

Second year core unit of study for the degrees in Mechanical and Aeronautical Engineering.

Syllabus Summary

Materials classification; understanding materials properties and their relation to structure as a function of forming methods and heat treatment processes; materials behaviour in service; selection criteria and case studies for engineering applications. Objectives

To understand the classification of engineering materials, and their properties in relation to microstructure.

Expected outcomes

Students should be able to appreciate the properties of a range of engineering materials and how and why these are connected with microstructures and forming and treatment methods.

 

Unit of Study Aims/Goals:

MECH2300 is your introductory course in engineering materials. It has no prerequisite subjects and is therefore intended for students with little or no previous background in engineering materials. A background in mathematics and science commensurate with a second year engineering undergraduate student is sufficient.

 

There are three key focus areas:

  1. Atomic structure of the solid state: atomic bonding, crystal structures, and crystal imperfections.
  2. Properties of materials and the relationship between properties and microstructure.
  3. The effects of heat treatment on microstructure and properties.

 

In order to attain these key understandings the aims of this subject are

  1. To gain understanding of the ways in which atoms are arranged in the solid state and of the ways in which their arrangement and the imperfections of their arrangement affect the macroscopic properties of a material.
  2. To gain understanding of the various types of mechanical properties of materials, how to measure and calculate them, and how to use these skills in engineering design and failure analysis.
  3. To gain understanding of the means by which the properties of materials can be manipulated via heat treatment, alloying, and other means.

 

In passing this subject you will then be able to apply these analysis and design skills in more advanced ways. You will have the ability to design, manipulate, and analyse materials in greater depth, and learn to understand and control more complex materials, in MECH3300, the third year materials subject.

 

Relationship between this UoS and University generic attributes

The University of Sydney has a set of generic attributes which it believes a graduate should attain upon completion of their degree which will provide them with the opportunity of being “more employable, more able to cope with change and more developed as people”. These attributes can be seen at http://www.usyd.edu.au/su/planning/policy/acad/102_grad.html.

This UoS will provide the following generic attributes

  1. Knowledge Skills – all attributes in this section will be dealt with in this course. In particular, to acquire a body of knowledge in materials engineering, application of materials engineering theory in familiar and unfamiliar situations, and  the ability to communicate this knowledge (especially in the written form). 
  2. Thinking Skills – all attributes in this section will be dealt with in this course. In particular, in the field of materials engineering, the ability to adopt a problem solving approach and to be able to account for decisions.
  3. Personal Skills – In particular to generate the capacity for further learning in the area of materials engineering.
  4. Personal Attributes – In particular the ability to value your own engineering judgments in the area of design with materials and gain a sense of the social responsibility involved in design with materials.

  5. Practical Skills – all attributes in this section will be dealt with in this course. Specifically, to be able to:

(a) use information technology as part of the learning process.
(b) collect, correlate, display, analyse and report observations in materials evaluation.
(c) apply experimentally-obtained results to new theoretical situations.
(d) test hypotheses experimentally.
(e) apply technical skills in materials design and evaluation.

Student Learning Outcomes:

The outcomes of this subject are:

  1. To be able to describe, in relatively simple terms, the crystal structure and associated crystal imperfections of materials, describing theoretically, schematically, and mathematically.
  2. To be able to describe, in relatively simple terms, the process of solid state diffusion in materials, describing theoretically, schematically, and mathematically.
  3. To be able to describe the main properties of materials, how to test for each, and how to analyse and calculate the results of a test. This encompasses mechanical, electrical, thermal, and magnetic properties.
  4. To be able to describe, in relatively simple terms, the concepts of mechanical properties of metals and how they are tested, and to relate the significance of this in terms of engineering design.
  5. To understand the basics of binary phase diagrams and to be able to use them in describing and measuring the effects of heat treatment on microstructure. The significance of metastability will be a key focus, particularly in relation to metallurgy.

 

Learning Situations

There will be two lectures per week where the theory, ideas, and engineering implementation to real systems will be discussed. The lectures will be held in:

l        Farrell Lecture Theatre 1 (Farrell LT) on Mondays at 12pm

l        Farrell Lecture Theatre 1 (Farrell LT) on Thursdays at 11am

You are required to attend one tutorial a week. Tutorials begin in week 2 and you can choose which tutorial to attend, but once you have registered for a particular room and time, you must not change to a different one without the permission of your tutor. The following are the tutorial times:

l        Mechanical Engineering Tutorial Room 3 on Tuesdays at 11AM

l        Electrical Engineering Tutorial Room 620 on Tuesdays at 11AM

l        Mechanical Engineering Tutorial Room 2 on Wednesdays at 11AM

l        Mechanical Engineering Tutorial Room 3 on Wednesdays at 11AM

l        Mechanical Engineering Tutorial Room 3 on Thursdays at 9AM

l        Mechanical Engineering Tutorial Room 4 on Thursdays at 9AM

l        Mechanical Engineering Tutorial Room 3 on Thursdays at 10AM

l        Mechanical Engineering Tutorial Room 4 on Thursdays at 10AM  

During the tutorial you will work through the allocated problems, seeking the assistance from your tutor as required. You will be expected to complete the pre-tutorial work before attending tutorials.

 

Laboratory

Laboratories will be held on Wednesday, Thursday, and Friday afternoons from 2PM to 5PM. Each student is required to attend only twice during the semester, once for the Mechanical Properties Laboratory, and once for the Weibull Strength Laboratory. Your specific two days will be allocated to you in the tutorials.

 


Assessment – Tasks:

There are four assignments. These are based on problems from the textbook. (Callister 6th Edition, see below).

  1. Assignment 1 is on structure of the solid state and diffusion. Callister problems 3.9, 3.15, 4.19, 5.11.
  2. Assignment 2 is on mechanical properties and phase diagrams. Callister problems 6.40, 7.18, 9.20, 9.24
  3. Assignment 3 is on electrical properties and semiconductors. Callister problems 18.2, 18.8, 18.10, 18.12.
  4. Assignment 4 is on dielectric, magnetic and thermal properties. Callister problems 18.54w, 19.9, 20.6, 20.23.

 

Assessment – Timetable:

 

No.

Component

Due Date

Weight

1

Assignment 1, structure of the solid state and diffusion

Week 3

5%

2

Assignment 2, mechanical properties and phase diagrams

Week 6

5%

3

Assignment 3, electrical properties and semiconductors

Week 9

5%

4

Assignment 4, dielectric, magnetic and thermal properties

Week 12

5%

5

Laboratory 1, mechanical properties of engineering materials

Report due 2 weeks after lab attendance

10%

6

Laboratory 2: Weibull strength of engineering materials

Report due 2 weeks after lab attendance

10%

7

Theory (Individual, written assessment of entire course)

Exam Period

60%

 

 

Assessment – Grade Attributes:

The following grade descriptors describe what is required from you to achieve the following grade levels.

 

Grade Level

Descriptor

Pass

         Students who aim for a Pass should be able to

        Understand the concepts of atomic structure and microstructure

        Identify the various properties of materials

        Use simple equations for problem solving and enumeration

        Be able to interpret phase diagrams

 

Credit

         Students who aim for a credit will have to accomplish the requirements of a Pass and should be able to

        Understand the complexities and their significance of atomic and microstructural modification techniques.

        Clearly describe the relevance of material properties, and their relative significance, in terms of design with materials.

        Manipulate simple equations in order to test new theories and be able to graph them accordingly in a clear and concise manner for communication purposes

        Explain and understand the assumptions behind phase diagrams: equilibrium, metastability, solution, and immiscibility, and their relationship with reality.

 

Distinction & High Distinction

         Students who aim for a distinction and higher will have to accomplish the requirements of a Credit and should be able to

        Describe in detail the various atomic and microstructural modification methods, their relative merits, and suggest other possibilities.

        Describe, in a wholistic manner, the overall relationship between the various strands of the course, within the context of responsible engineering design: atomic structure and microstructure, properties, heat-treatment and chemical composition.

        Manipulate equations from first principles to new systems.

 

 


Unit of Study Program:

The following program is indicative only.

 

Lecture

Description (Dr Ruys will give lectures 1-13, Dr Parakala Lectures 14-26).

Tutorials

1

Objectives, structure and assessment of the course

No tutorials in

week 1

2

Introduction to materials (Chapter 1)

3

Introduction to materials (Chapter 1)

Tutorial 1

Callister Problems

3.4, 3.6, 4.5, 4.30

 

4

Structure of crystalline solids (Chapter 3)

5

Imperfections in solids (Chapter 4)

6

Diffusion in solids and engineering applications (Chapter 5)

 

Assignment #1 due

 

7

Mechanical properties of metals (Chapter 6)

Tutorial 2

Callister Problems

5.8, 5.12, 6.7, 6.29

8

Mechanical properties of metals (Chapter 6)

9

Dislocation and strengthening mechanisms (Chapter 7)

10

Dislocation and strengthening mechanisms (Chapter 7)

11

Phase diagrams (Chapter 9)

Tutorial 3

Callister Problems

9.5, 9.7, 9.9

12

Phase diagrams (Cont'd Chapter 9)

 

Assignment #2 due

13

Annealing, heat treatment, and precipitation hardening (Chapter 10,11)

14

Electrical properties of materials (Chapter 18)

15

Electrical properties of materials (Chapter 18)

Tutorial 4

Callister Problems

18.1, 18.11, 18.30

16

Semiconductors (Chapter 18)

17

Semiconductors (Chapter 18)

18

Dielectrical Behavior (Chapter 18)

 

Assignment #3 due

Tutorial 5

Callister Problems

18.56w, 18.59w

19

Dielectrical Behavior (Chapter 18)

20

Magnetic Properties (Chapter 20)

21

Magnetic Properties (Chapter 20)

22

Magnetic Properties (Chapter 20)

Tutorial 6

Callister Problems

19.12, 20.1

23

Thermal Properties (Chapter 19)

24

Thermal Properties (Chapter 19)

 

Assignment #4 due

25

Revision

26

Revision

 

 

Unit of Study References:

  1. The textbook by WD Callister, Jr: Materials Science and Engineering, 6th Edition will be used.
  2. Some lecture notes are also on the website http://www.camt.usyd.edu.au/education/MECH2300
  3. Printed lecture notes are available at the University Copy Centre

 

Further, information on the course and on the laboratories is also on the website http://www.camt.usyd.edu.au/education/MECH2300

 

Staff Contact Information

 

Position

Name

Email

Telephone

Room Number

Lecturer

Coordinator

Dr Andrew Ruys

a.ruys@aerommech.usyd.edu.au

9351 8610

Rm 521 Mechanical

Lecturer/Tutor

Dr Padmaja Parakala

paddy.parakala@aeromech.usyd.edu.au

9351 3723

Rm 515Mechanical

Demonstrator

Philip Boughton

boughton@aeromech.usyd.edu.au

 

Rm 342 Mechanical

Demonstrator

Elizabeth Kolos

Elizabeth.Kolos@aeromech.usyd.edu.au

 

Rm 342 Mechanical

Tutor

Ryan Prasad

npra7729@mail.usyd.edu.au

 

 

Tutor

Sav Shimada

sshi4720@mail.usyd.edu.au

 

 

 


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